Metrohm 766 IC Sample Processor Manuel d'utilisateur

CH-9101 Herisau/SwitzerlandTel. ++41 71 353 85 85Fax ++41 71 353 89 01Internet www.metrohm.chE-Mail [email protected] IC Sample ProcessorDES FUSIBLE

1.3 Information about the Instructions for Use766 IC Sample Processor51.3 Information about the Instructions for UsePlease read through these Instru

5.2 RS232 interface766 IC Sample Processor955.2.3 TriggerTriggers initiate an action at the 766 IC Sample Processor, e.g. se-quence start or data tr

5 Interfaces766 IC Sample Processor965.2.4 Status messagesTo ensure appropriate control of an external control unit is possible, itmust also be poss

5.2 RS232 interface766 IC Sample Processor975.2.5 Error messagesError messages ‘EXXX’ are appended to the status message and sepa-rated from this by

5 Interfaces766 IC Sample Processor985.2.6 Remote control commandsThe remote control tree can be divided into the following mainbranches:& RootÃ

5.2 RS232 interface766 IC Sample Processor99Object Meaning Entry range/Selection³Ã.FinalSeq Final sequence –³ Ã.1 Line number of the command –³ ³ Ã.C

5 Interfaces766 IC Sample Processor100Object Meaning Entry range/Selection³ ³³ Ã.R1O1Off Offset in 1/10-ang. degrees for positions in row 1 0…3599³ Ã

5.2 RS232 interface766 IC Sample Processor101Object Meaning Entry range/Selection ³ Ã.Outputs Remote outputs ³ À.Status ³ Status of the 14 outp

5 Interfaces766 IC Sample Processor102Object Meaning Entry range/Selection³ ³³ Ã.UserMeth Locking of method memory functions on, off³ ³ Ã.Recall Lock

5.2 RS232 interface766 IC Sample Processor103Object Meaning Entry range/Selection&Assembly&Assembly Assembly control –³Ã.Sample Current sampl

5 Interfaces766 IC Sample Processor104Object Meaning Entry range/Selection&Diagnose&Diagnose Diagnosis (see section 6.4)³Ã.Init Initializatio

1 Introduction766 IC Sample Processor61.3.2 Notation and pictogramsThe following notations and pictograms (symbols) are used in these In-structions

5.2 RS232 interface766 IC Sample Processor1055.2.7 Data transmission protocolThe RS232 interface of the 766 IC Sample Processor is configured asDTE

5 Interfaces766 IC Sample Processor1065.2.8 HandshakeNo Handshake (none)The 766 IC Sample Processor neither checks handshake inputs (CTS,DSR, DCD) n

5.2 RS232 interface766 IC Sample Processor107766 IC Sample Processor as sender:LFDCDCTSTxDDCDCTSTxDDSR DSRRTS RTSThe data flow can be interrupted by

5 Interfaces766 IC Sample Processor108766 IC Sample Processor as sender:RxDTxDXOFFLFXONSoftware handshake with line stop (SWline)Handshake inputs are

5.2 RS232 interface766 IC Sample Processor1095.2.9 Pin assignmentRS232C interface externalTransmitted Data (TxD)If no data transmission takes place,

5 Interfaces766 IC Sample Processor1105.2.10 RS232 error rectificationProblem Questions for corrective actionNo characters can be re-ceived on an at

6.1 Error messages766 IC Sample Processor1116 Appendix6.1 Error messagesWhen an error occurs the execution of the active command is inter-rupted an

6 Appendix766 IC Sample Processor112Error messageCause* changer low power The power supply cannot deliverenough power for the simultaneousoperation o

6.2 Technical data766 IC Sample Processor1136.2 Technical dataLiftLift path ca. 125 mmLoad ca. 30 NStroke speed adjustable, 3…12 mm/sTurntableTurnin

6 Appendix766 IC Sample Processor114Safety specificationsConstruction / Testing According to IEC 1010 / EN 61010 / UL 3101-1,protection class 1, degr

1.4 Support documentation766 IC Sample Processor71.4 Support documentation1.4.1 Application BulletinsThe «Application Bulletin» is a collection of

6.3 Maintenance and servicing766 IC Sample Processor1156.3 Maintenance and servicing6.3.1 Maintenance by Metrohm serviceMaintenance of the 766 IC S

6 Appendix766 IC Sample Processor1166.3.3 Replacing the pump tubingPump tubings are consumable material with a limited lifetime andshould be replace

6.4 Diagnosis766 IC Sample Processor1176.4 Diagnosis6.4.1 General InformationThe 766 IC Sample Processor is a very precise and reliable control in-

6 Appendix766 IC Sample Processor118Required Instruments:Only required, if the RS232 or remote interface is to be checked:• 3.496.8550 Test plug (on

6.4 Diagnosis766 IC Sample Processor1196.4.3 Working memory (RAM)This diagnosis step completes a non-destructive test over the entirerange of the RA

6 Appendix766 IC Sample Processor120• The test can be exited with the <QUIT> or <STOP> keys.diagnosis>display contrast test• <ENT

6.4 Diagnosis766 IC Sample Processor121Key code tableCode Key Code Key0 16 <7 / SAMPLE>1 <HOLD / LEARN> 17 <4 / PUMP>2 <STOP>

6 Appendix766 IC Sample Processor1226.4.7 RS232 interfaceThis diagnosis step tests the functionality of the serial interface.• Prepare instrument f

6.4 Diagnosis766 IC Sample Processor1236.4.9 Beeper• Prepare instrument for diagnosis (see section 6.4.2).• If necessary, press <ê> several

6 Appendix766 IC Sample Processor124• <ENTER>The test reads the code continuously and displays it immediately. For representation on thescreen

1 Introduction766 IC Sample Processor8• Protection against static chargesElectronic components are sensitive to static charging and can bedestroyed

6.5 Initialize data memory766 IC Sample Processor125• Prepare instrument for diagnostic test (see section 6.4.2).• If need be, press <9> key

6 Appendix766 IC Sample Processor1266.6 Validation / GLPGLP (Good Laboratory Practice) requirements include the periodiccheck of analytical instru

6.7 Warranty and conformity766 IC Sample Processor1276.7 Warranty and conformity6.7.1 WarrantyThe warranty on our products is limited to defects th

6 Appendix766 IC Sample Processor1286.7.2 EU Declaration of conformityEU Declaration of ConformityThe METROHM AG company, Herisau, Switzerland hereb

6.7 Warranty and conformity766 IC Sample Processor1296.7.3 Certificate of conformity and system validationCertificate of Conformity and System Valid

6 Appendix766 IC Sample Processor1306.8 Standard equipmentSubject to changes !All dimensions are given in mm.The 2.766.0010 IC Sample Processor incl

6.8 Standard equipment766 IC Sample Processor131Quant. Order No. Description1 6.2142.010 Keyboardfor 766 IC Sample Processor1 6.2621.060 Open-end spa

6 Appendix766 IC Sample Processor132Quant. Order No. Description1 8.766.1003 Instructions for Use (English)for 766 IC Sample Processor1 8.766.1013 Qu

6.10 Index766 IC Sample Processor1336.10 IndexAActions at manual stop... 60Adaptor (6.2125.120)Interconnection

6 Appendix766 IC Sample Processor134FFilling two sample loops ... 17Final sequence...

2.1 Setting up the instrument766 IC Sample Processor92 Installation2.1 Setting up the instrument2.1.1 PackagingThe 766 IC Sample Processor is supp

6.10 Index766 IC Sample Processor135Method parameters... 58Method processing ...

6 Appendix766 IC Sample Processor136Pump drive 1414Figure ... 3Pump status...

6.10 Index766 IC Sample Processor137Special position... 30,77special position...

6 Appendix766 IC Sample Processor138Keys< < >... 49< > >...

2 Installation766 IC Sample Processor102.2 Mains connectionFollow the instructions below for connecting to the power supply. Ifthe instrument is ope

2.2 Mains connection766 IC Sample Processor11262625252424220 -- 240 V 100 -- 120 V 220 -- 240 V 100 -- 120 V Fig. 3: Setting the mains voltage2.2.2

2 Installation766 IC Sample Processor122.3 Attaching the accessoriesFor attaching the accessories at the 766 IC Sample Processor, pro-ceed in the or

2.3 Attaching the accessories766 IC Sample Processor132.3.4 Installing the splash protectionTo avoid any danger of injury by the needle, the 6.2751.

2 Installation766 IC Sample Processor14224455667788 Fig. 6: Needle installationIf you are using the 6.1835.000 PEEK needle, the sample tubes maynot

Table of contents766 IC Sample ProcessorITable of contents1 Introduction...

2.3 Attaching the accessories766 IC Sample Processor1527273333323222 Fig. 8: Adjusting the sample rack2Move to adjusting positionPress <MOVE>,

2 Installation766 IC Sample Processor162.3.8 Tubing connections 766 – 733For transferring the sample from the 766 IC Sample Processor to theinjectio

2.3 Attaching the accessories766 IC Sample Processor1788 3535 1010 3636 1313 1515 3636 3535 18181717 343466 Fig. 9: Installing the pump tubing66 PEE

2 Installation766 IC Sample Processor182.3.9 Tubing connections 766 – 754If the 766 IC Sample Processor is used for an IC system with sampledialysis

2.4 Connection of devices to the remote interface766 IC Sample Processor192.4 Connection of devices to theremote interface2.4.1 General information

2 Installation766 IC Sample Processor202.4.3 IC system without suppressionThe 766 IC Sample Processor is connected to an IC system withoutsuppressio

2.4 Connection of devices to the remote interface766 IC Sample Processor212.4.5 IC system with suppression with PC as "Master"The 766 IC S

2 Installation766 IC Sample Processor222.4.7 IC system with sample dialysisThe 766 IC Sample Processor is connected to an IC system with sam-ple dia

2.5 Connection of devices to the RS232 interface766 IC Sample Processor232.5 Connection of devices to the RS232interface2.5.1 General information o

2 Installation766 IC Sample Processor242.5.2 Connection of a printerPrinters with the following printer drivers may be connected:IBM IBM Proprinter

Table of contents766 IC Sample ProcessorII2.4 Connection of devices to the remote interface... 192.4.1 General information on r

2.5 Connection of devices to the RS232 interface766 IC Sample Processor25Printer Cable RS232 settings Settings on printerCitizenIDP562-RS6.2125.050 b

2 Installation766 IC Sample Processor26

3.1 Prerequisites / Preparations766 IC Sample Processor273 Operating tutorialIn order to become acquainted with the 766 IC Sample Processor and itsm

3 Operating tutorial766 IC Sample Processor283.2 ConfigurationCONFIGENTERTOWERSELECT• The dialog language can be set in the configuration menu. Pr

3.3 Rack configuration766 IC Sample Processor29RESETCLEAR• At the end of this basic configuration the 766 IC Sample Processormust be turned off and

3 Operating tutorial766 IC Sample Processor30<ENTER>>rack definitions 2work position 71 mm• In any case don’t forget to confirm t

3.4 Methods766 IC Sample Processor313.4 MethodsUSERMETHOD<ENTER>TOWERSELECT<ENTER>• Now open the user method menu by pressing <USER

3 Operating tutorial766 IC Sample Processor32<ENTER><ê>START<QUIT>parameters>start sequence• In the submenu '>start seq

3.5 "Tracing"766 IC Sample Processor33 <ENTER>• Now move the lift into the desired position with the <ê> and <é>keys. Y

3 Operating tutorial766 IC Sample Processor34<QUIT><ê><ENTER>>sample sequence 9 NOP• An empty line with a 'NOP'-entry

Table of contents766 IC Sample ProcessorIII4.4.3 Setting the sample position ... 714.4.4 Pump contro

4.1 Fundamentals of operation766 IC Sample Processor354 OperationThis section provides a detailed description of the operation of the766 IC Sample P

4 Operation766 IC Sample Processor364.1.2 KeyboardSC Controller******** counter 1/999PUMP- readyTOWER 1 TOWER 2 LEARNPARAMHOMEENDINSE

4.1 Fundamentals of operation766 IC Sample Processor374.1.3 Overview of key functionsKey Normal state Edit modeCONFIGOpen the configuration menu• T

4 Operation766 IC Sample Processor38Key Normal state Edit modeENDLift in work position• The <END> key runs the lift intothe work position.• T

4.1 Fundamentals of operation766 IC Sample Processor39Key Normal state Edit modeTurn rack right• The <è> key turns the samplerack one position

4 Operation766 IC Sample Processor40Key Normal state Edit modeRESETCLEARInitialization of the IC SampleProcessor• The <RESET> key serves toini

4.1 Fundamentals of operation766 IC Sample Processor41Key Normal state Edit modeENTERAccept data, next line• The <ENTER> key accepts thevalue

4 Operation766 IC Sample Processor42Key Normal state Edit mode9LIFTPositioning the lift• Raises or lowers the lift to apredefined position. These po

4.1 Fundamentals of operation766 IC Sample Processor43Key Normal state Edit mode2CTRLInterface control• Controlling of external instrumentsvia the r

4 Operation766 IC Sample Processor44Key Normal state Edit mode• "<" serves also for shifting thechain of characters to chose from,i.e.

Table of contents766 IC Sample ProcessorIV6.4 Diagnosis... 1176.4

4.1 Fundamentals of operation766 IC Sample Processor45Key Normal state Edit modeSTOPStop process and peripheralinstruments• The <STOP> key ter

4 Operation766 IC Sample Processor464.1.4 Instrument dialogThe instrument dialog of the 766 IC Sample Processor is organized inthe form of so-called

4.1 Fundamentals of operation766 IC Sample Processor47Kex title>Submenu 1QUITKEYENTERENTERENTERKEYNormal stateQUITKey title>Submenu n>Submen

4 Operation766 IC Sample Processor484.1.5 Data entryEdit lineIn a menu line or a sequence one or two parameters respectively canbe entered. A blinki

4.1 Fundamentals of operation766 IC Sample Processor494.1.6 Text entryThe text editor can be used when text entry is provided.Numbers can be entered

4 Operation766 IC Sample Processor50Scheme>store methodmethod:ÛÛABCDEFGHIJ...abcd...1234...*%&/()=... 2x ">">store methodmetho

4.2 Basic settings766 IC Sample Processor514.2 Basic settings4.2.1 Configuration – <CONFIG> keyCONFIGThe <CONFIG> is used for the entry

4 Operation766 IC Sample Processor52>auxiliariesbeeper: ONON,OFFAcoustic warning signalON Acoustic warning signal in case of errorme

4.2 Basic settings766 IC Sample Processor53>rack definitions 2type: M129-2M129-2……Type description of the rack<SELECT> enab

4 Operation766 IC Sample Processor54configuration>RS232 settingsSettings for RS232 interfaceFor further details on the RS232 interface, see sectio

1.1 Instrument description766 IC Sample Processor11 Introduction1.1 Instrument descriptionThe 766 IC Sample Processor can be used for automating io

4.2 Basic settings766 IC Sample Processor554.2.2 Locking keyboard functionsSwitch on +CONFIGCertain domains of the user dialog can be made inac-cess

4 Operation766 IC Sample Processor56>keyboard options>user methodsSubmenu for locking method storage func-tions>user methodslock method reca

4.3 Methods766 IC Sample Processor574.3 Methods4.3.1 Structure of a methodA method consists of the following parts:• Number of samples to be proce

4 Operation766 IC Sample Processor584.3.2 Method parameters – <PARAM> keyPARAMThe <PARAM> key combines the most important parameter sett

4.3 Methods766 IC Sample Processor59parameters>start sequenceStart sequence of a sample seriesThe processing sequence entered here is executed onc

4 Operation766 IC Sample Processor60parameters>manual stopActions at manual stopThe following entries define the commands or signals that aretrans

4.3 Methods766 IC Sample Processor614.3.4 LEARN modeHOLDLEARNWhen editing a method, the parameters of a command are most easilydetermined experiment

4 Operation766 IC Sample Processor624.3.6 Commands for sequencesThe following commands are programmable within a sequence. Mostof them are also avai

4.3 Methods766 IC Sample Processor63LIFT9LIFT>sample sequence 3 LIFT: 1 : rest mmwork,rinse,shift,special,rest,0…125 mmPosition the liftRaisin

4 Operation766 IC Sample Processor64Predefined bit patterns are supported which can be selected by shortnames (e.g. 'Ready1' or 'End2&

1 Introduction766 IC Sample Processor21.2 Parts and controlsDES FUSIBLES DE 250VUSE ONLY WITH 250VUNIQUEMENT AVECFUSES/EMPLOYER100-120V220-240V11Met

4.3 Methods766 IC Sample Processor65More detailed information about the syntax can be found in the Instruc-tions for Use of the instrument from which

4 Operation766 IC Sample Processor66Data (= character string) can be sent to instruments connected via theserial RS232 interface.Make sure that the t

4.3 Methods766 IC Sample Processor674.3.7 Process controlSTARTWith <START> a method is started from the normal state. If there is nomanual int

4 Operation766 IC Sample Processor684.3.8 User defined methodsUSERMETHODThe <USER METHOD> key is used for the management of user de-fined meth

4.3 Methods766 IC Sample Processor69methods>delete methodDeletion of methods>delete methodmethod: ********8 ASCII charactersSelection o

4 Operation766 IC Sample Processor704.4 Manual operation4.4.1 Turning the sample rack / Positioning the samples Using the <ç> and <è>

4.4 Manual operation766 IC Sample Processor714.4.3 Setting the sample position7SAMPLEmanual operationSAMPLE: = 11…999Define current sam

4 Operation766 IC Sample Processor724.4.6 Interface control2CTRLmanual operationCTL:Rm : INITRm,RS INITINIT 732PROG R/S 1PRO

4.4 Manual operation766 IC Sample Processor7344.4.4.7 .7 Print out reports.<PRINT******** counter 1/128Print: paramallconfigparamus

4 Operation766 IC Sample Processor74Example of "param" report 'pa766 IC Sample Proc. 0100 5.766.0010parameters method

1.2 Parts and controls766 IC Sample Processor311 Splash protection(6.2751.040)Must be installed always inoperation!1515 Contact pressure leverFor adj

4.5 Sample racks766 IC Sample Processor754.5 Sample racks4.5.1 Standard rack (6.2041.430)Metrohm delivers the following standard sample rack for th

4 Operation766 IC Sample Processor76Magnets insertedIn this examplethe code is:000110Rack bottom viewIn order to assign a certain sample rack for dif

4.5 Sample racks766 IC Sample Processor77The rack Type serves for the assignment to a position table internal tothe instrument, in which the position

4 Operation766 IC Sample Processor784.5.4 Special beakersSpecial beakers are reserved positions in a sample rack. 0 to 8 specialbeakers can be defin

4.6 Standard methods766 IC Sample Processor794.6 Standard methodsThe following pages contain the listing of standard user methods in-cluded with the

4 Operation766 IC Sample Processor80Settings in the «IC Metrodata» programDefinition of IC method (analysis time, start parameters for IC instru-ment

4.6 Standard methods766 IC Sample Processor81Settings in the «IC Metrodata» programDefinition of IC method (analysis time, start parameters for IC in

4 Operation766 IC Sample Processor82Settings for 732 IC DetectorSetting the measurement parameters.Settings in the «IC Metrodata» programDefinition o

4.6 Standard methods766 IC Sample Processor83Settings for 732 IC DetectorSetting the measurement parameters.Settings in the «IC Metrodata» programDef

4 Operation766 IC Sample Processor84Settings in the «IC Metrodata» program1. Definition of anion method for channel 1 (analysis time, start pa-ramet

1 Introduction766 IC Sample Processor49929293030313132322020Made by Metrohm Herisau SwitzerlandRS 232 KeyboardType 1.766.2929131311292920202929191928

4.6 Standard methods766 IC Sample Processor85 7 CTL:Rm: STEP MSM 753 8 PUMP 1.1 : 150 s 9 CTL:Rm: ZERO 1 10 CTL:Rm:

4 Operation766 IC Sample Processor864.6.7 Method "Preconc"ApplicationPreconcentration of samples with very low concentrations in an pre-co

4.6 Standard methods766 IC Sample Processor87>final sequence>changer settings rack number 0 lift rate 1 12 mm/s s

4 Operation766 IC Sample Processor88>final sequence 1 CTL:Rm: PUMP R/S 1>changer settings rack number 0 lift rate 1

5.1 Remote interface766 IC Sample Processor895 Interfaces5.1 Remote interfacePeripheral instruments connected such as 732 IC Detector, 709 ICPump,

5 Interfaces766 IC Sample Processor90For the 766 IC Sample Processor, the output lines 11–13 and the inputline 7 are occupied for the control of the

5.1 Remote interface766 IC Sample Processor91Input linesThe 8 input lines of the remote socket are queried during method proc-essing with the "

5 Interfaces766 IC Sample Processor92CTL commandsParameter Bit pattern Function SignalINIT 00000000000000 initializes the remote interface staticINIT

5.2 RS232 interface766 IC Sample Processor935.2 RS232 interface5.2.1 General rules for remote controlThe 766 IC Sample Processor is equipped with t

5 Interfaces766 IC Sample Processor945.2.2 Call-up of objectsA section from the object tree is shown below:Language ProgAuxConfig&RootRSsetModeN