Metrohm 820 IC Separation Center Manuel d'utilisateur

819 IC Detector 820 IC Separation Center 5.819.0010 Program Instructions for Use8.819.1013 CH-9101 Herisau/Switzerland E-Mail [email protected]

1 Introduction 819 IC Detector / 820 IC Separation Center 2 1.1.2 820 IC Separation Center The 820 IC Separation Center is a thermally and elec

6 Appendix 819 IC Detector / 820 IC Separation Center 92 6.2 Scope of delivery Subject to changes ! All dimensions are given in mm. 6.2.1 819

6.2 Scope of delivery 819 IC Detector / 820 IC Separation Center 932.819.0110 IC Detector Quant. Order-No. Description 1 1.819.0010 819 IC D

6 Appendix 819 IC Detector / 820 IC Separation Center 94 0.25 1⁄16" 6 9 6.2.2 820 IC Separation Center The 820 IC Separation Center is avai

6.2 Scope of delivery 819 IC Detector / 820 IC Separation Center 951 6.2027.040 Column holder diameter d = 11.3 mm 42d 1 6.2027.050 Column holder

6 Appendix 819 IC Detector / 820 IC Separation Center 96 0.25 1⁄16" 6 9 2.820.0220 IC Separation Center Quant. Order-No. Description 1

6.2 Scope of delivery 819 IC Detector / 820 IC Separation Center 970.25 1⁄16"6 94 6.2744.040 PEEK coupling for the connection of 1⁄16" c

6 Appendix 819 IC Detector / 820 IC Separation Center 98 1 6.2027.030 Column holder diameter d = 8.5 mm 42d 1 6.2027.040 Column holder diameter d

6.2 Scope of delivery 819 IC Detector / 820 IC Separation Center 990.25 1⁄16"6 91 8.819.1013 Instructions for Use (English) for 820 IC Sep

6 Appendix 819 IC Detector / 820 IC Separation Center 100 0.25 1⁄16" 6 9 1 6.2744.070 PEEK compression fitting-(short) for the connection

6.2 Scope of delivery 819 IC Detector / 820 IC Separation Center 1010.25 1⁄16"6 92 6.2744.020 Coupling 1⁄16" – Luer Coupling for connect

1.1 Instrument description 819 IC Detector / 820 IC Separation Center 3 1.1.3 Schematic arrangement of the IC systems The 819 IC Detector and 820

6 Appendix 819 IC Detector / 820 IC Separation Center 102 1 6.2027.050 Column holder diameter d = 15.0 mm 42d 2 6.2744.010 PEEK compression fit

6.3 Optional accessories 819 IC Detector / 820 IC Separation Center 1036.3 Optional accessories 6.3.1 Accessories for 820 IC Separation Center Or

6 Appendix 819 IC Detector / 820 IC Separation Center 104 6.2821.090 Aspirating filter PE 20 µm For 6.1834.000 Aspirating tubing (sup-plied with

6.3 Optional accessories 819 IC Detector / 820 IC Separation Center 1056.3.3 Cable Order No. Description 6.2115.070 Remote Connection cable Con

6 Appendix 819 IC Detector / 820 IC Separation Center 106 6.4 Validation / GLP GLP (Good Laboratory Practice) requires, among other things, that

6.5 Warranty and Conformity 819 IC Detector / 820 IC Separation Center 1076.5 Warranty and Conformity 6.5.1 Warranty The warranty on our products

6 Appendix 819 IC Detector / 820 IC Separation Center 108 6.5.2 Declaration of Conformity This is to certify the conformity to the standard sp

6.5 Warranty and Conformity 819 IC Detector / 820 IC Separation Center 1096.5.3 Declaration of Conformity This is to certify the conformity to t

6 Appendix 819 IC Detector / 820 IC Separation Center 110 6.5.4 Quality Management Principles Metrohm Ltd., CH-9101 Herisau, Switzerland CH-910

6.6 Index 819 IC Detector / 820 IC Separation Center 1116.6 Index 8 818 IC Pump Connection at 819 ... 29 Electrical

1 Introduction 819 IC Detector / 820 IC Separation Center 4 1.2 Parts and controls In this Section you will find the numbers and designations of

6 Appendix 819 IC Detector / 820 IC Separation Center 112 Connection 25 Figure ... 8 Pin assignmen

6.6 Index 819 IC Detector / 820 IC Separation Center 113Figure... 40, 43 Mounting...

6 Appendix 819 IC Detector / 820 IC Separation Center 114 Practical notes ... 67 Pulsations...

6.6 Index 819 IC Detector / 820 IC Separation Center 115ValveA ... 58, 64 ValveB ...

1.2 Parts and controls 819 IC Detector / 820 IC Separation Center 5 Fig. 3: Rear of the 819 IC Detector 2 Mains switch For switching instrument o

1 Introduction 819 IC Detector / 820 IC Separation Center 6 1.2.2 820 IC Separation Center Fig. 4: Front of the 820 IC Separation Center 11 Mai

1.2 Parts and controls 819 IC Detector / 820 IC Separation Center 7 Fig. 5: Rear of the 820 IC Separation Center 15 15 16 18 20 17 19 33 34 15 1

1 Introduction 819 IC Detector / 820 IC Separation Center 8 14Feedthrough for sample, eluent, suppressor re-agent,… 15Knurled screw for fastening

1.2 Parts and controls 819 IC Detector / 820 IC Separation Center 9 Column heating Fig. 6: Column heating closed 35Feedthrough for the capillary

1 Introduction 819 IC Detector / 820 IC Separation Center 10 1.3 Information on the Instructions for Use Please read through these Instructions

1.3 Information on the Instructions for Use 819 IC Detector / 820 IC Separation Center 111.3.2 Notation and pictograms The following notations and

1 Introduction 819 IC Detector / 820 IC Separation Center 12 1.4 Safety notes While electrical safety in the handling of the 819 IC Detector and

2.1 Setting up the instrument 819 IC Detector / 820 IC Separation Center 132 Installation 2.1 Setting up the instrument 2.1.1 Packaging 819 IC De

2 Installation 819 IC Detector / 820 IC Separation Center 14 In one-channel operation, the 818 IC Pump, 820 IC Separation Center and 819 IC Dete

2.2 Installation of accessories 819 IC Detector / 820 IC Separation Center 152.2 Installation of accessories 2.2.1 Insert detector block In order

2 Installation 819 IC Detector / 820 IC Separation Center 16 Fig. 8: Connection Detector 819 – 2.820.0X10/2.820.0X30 2 Connect detector bloc

2.2 Installation of accessories 819 IC Detector / 820 IC Separation Center 17• Replace rear panel 21 and screw to the 820 IC Separation Center usin

2 Installation 819 IC Detector / 820 IC Separation Center 18 2.2.2 Connection of column heating The instrument versions 2.820.02X0 of the IC Sep

2.2 Installation of accessories 819 IC Detector / 820 IC Separation Center 19Fig. 11: Connection 820 – column heating 2.2.3 Connection of syringe

2 Installation 819 IC Detector / 820 IC Separation Center 20 2.3 Electrical connection 2.3.1 Connection to 830 IC Interface The instruments are

2.3 Electrical connection 819 IC Detector / 820 IC Separation Center 211 Connect 819 to 820 • Use 6.2125.090 Cable to connect Connection 10 “IC

CH-9101 Herisau/Switzerland E-Mail [email protected] Internet www.metrohm.com 819 IC Detector 820 IC Separation Center 5.819.0010 Program

2 Installation 819 IC Detector / 820 IC Separation Center 22 Separate control of the Separation Center Alternatively you have the possibility of

2.3 Electrical connection 819 IC Detector / 820 IC Separation Center 232 Connect 820 to 830 Control lines to switch the valve to FILL or INJECT

2 Installation 819 IC Detector / 820 IC Separation Center 24 2 Connect 819 to PC • Use 6.2125.110 Cable to connect Connection 9 “RS 232” of t

2.4 Mains connection 819 IC Detector / 820 IC Separation Center 252.4 Mains connection Follow the instructions below for connecting to the power

2 Installation 819 IC Detector / 820 IC Separation Center 26 Fig. 15: Setting the mains voltage Fuses One of the two fuses 0.63 A/slow-blow for

2.5 Software-installation 819 IC Detector / 820 IC Separation Center 272.4.2 820 IC Separation Center If an 820 IC Separation Center is included i

2 Installation 819 IC Detector / 820 IC Separation Center 28 2.6 Capillary connections Some of the connections under high pressure between the fe

2.7 Connection of 818 IC Pump 819 IC Detector / 820 IC Separation Center 292.7 Connection of 818 IC Pump 2.7.1 Electrical connection For operation

2 Installation 819 IC Detector / 820 IC Separation Center 30 nectors supplied or two 6.2744.010 PEEK compression fittings can be used. The flow d

2.7 Connection of 818 IC Pump 819 IC Detector / 820 IC Separation Center 312.7.4 Connection to injection valve It is recommended to use 6.1831.010

Teachware Metrohm AG Oberdorfstrasse 68 CH-9101 Herisau [email protected] 2nd Edition 2004 These instructions are protected by copyright. All

2 Installation 819 IC Detector / 820 IC Separation Center 32 3 Installation of the capillary in the IC Separation Center • Unscrew the four k

2.8 Precolumns 819 IC Detector / 820 IC Separation Center 332.8 Precolumns The use of easily exchangeable precolumns protects the separating colum

2 Installation 819 IC Detector / 820 IC Separation Center 34 2.9 Separating columns and suppressor module 2.9.1 General information on separatin

2.9 Separating columns and suppressor module 819 IC Detector / 820 IC Separation Center 352.9.2 Installing a separating column in the column heati

2 Installation 819 IC Detector / 820 IC Separation Center 36 1 Open column heating • Open the two knurled screws 36 and remove cover 37 of t

2.9 Separating columns and suppressor module 819 IC Detector / 820 IC Separation Center 372.9.3 Selection of the sample loop Selection of the samp

2 Installation 819 IC Detector / 820 IC Separation Center 38 To avoid contamination of the suppressor module by foreign particles or bacterial gr

2.9 Separating columns and suppressor module 819 IC Detector / 820 IC Separation Center 39 2.9.5 One-channel system without suppressor module Ma

2 Installation 819 IC Detector / 820 IC Separation Center 40 53Separating column 56Detector block 57Inlet capillary for detector block fixed moun

2.9 Separating columns and suppressor module 819 IC Detector / 820 IC Separation Center 412.9.6 Two-channel system without suppressor module Ma

Table of contents 819 IC Detector / 820 IC Separation Center I Table of contents 1 Introduction...

2 Installation 819 IC Detector / 820 IC Separation Center 42 2.9.7 One-channel system with suppressor module Make sure that the connection sep

2.9 Separating columns and suppressor module 819 IC Detector / 820 IC Separation Center 4348PEEK capillary (6.1831.010) to 818 IC Pump 49Pulsation

2 Installation 819 IC Detector / 820 IC Separation Center 44 3 Connect column to suppressor module (Suppressor connection 1) • Cut inlet capi

2.9 Separating columns and suppressor module 819 IC Detector / 820 IC Separation Center 455 Connect suppressor module to detector block (Suppres

2 Installation 819 IC Detector / 820 IC Separation Center 46 8 Suppressor connection 3: H2O • Pull inlet capillary 68 (marked with "H2S

2.9 Separating columns and suppressor module 819 IC Detector / 820 IC Separation Center 472.9.8 Two-channel system with suppressor module Make s

2 Installation 819 IC Detector / 820 IC Separation Center 48 In order to operate a 2-channel Separation Center with chemical sup-pression a 2.833

2.9 Separating columns and suppressor module 819 IC Detector / 820 IC Separation Center 492 Check 818 IC Pump • Check that the aspiration capi

3 Operation 819 IC Detector / 820 IC Separation Center 50 3 Operation The operation of 819 IC Detector and 820 IC Separation Center is made compl

3.1 819 IC Detector 819 IC Detector / 820 IC Separation Center 51 Conductivity Live display of measured conductivity (auto-zero value) in µS/cm.

Table of contents 819 IC Detector / 820 IC Separation Center II 3 Operation ...50 3.1 819 IC

3 Operation 819 IC Detector / 820 IC Separation Center 52 Zero <ON> Triggers the auto-zero function. Zero <OFF> Switch off the auto

3.1 819 IC Detector 819 IC Detector / 820 IC Separation Center 53If the measured conductivity value exceeds ±180% of the set full-scale range, the

3 Operation 819 IC Detector / 820 IC Separation Center 54 Full scale The full scale range (operating range) sets the desired sensitivity for the

3.1 819 IC Detector 819 IC Detector / 820 IC Separation Center 55 Ion Combination of polarity and temperature coeffi-cient: Anion polarity = +,

3 Operation 819 IC Detector / 820 IC Separation Center 56 Damping Electronic damping of the analog output Selection: on, off Damping to reduce d

3.1 819 IC Detector 819 IC Detector / 820 IC Separation Center 57Program On the Program subpage, program steps including time, program in-structio

3 Operation 819 IC Detector / 820 IC Separation Center 58 Instruction Parameter entry Meaning ValveA fill, inject Switch injection valve A to &

3.1 819 IC Detector 819 IC Detector / 820 IC Separation Center 59<Add> Add new remote command. <Delete> Delete selected remote comma

3 Operation 819 IC Detector / 820 IC Separation Center 60 3.2 820 IC Separation Center 3.2.1 820 IC Separation Center icon 3.2.2 "820 IC

3.2 820 IC Separation Center 819 IC Detector / 820 IC Separation Center 61Manual The Manual tab of the 820 IC Separation Center window is only avai

Table of contents 819 IC Detector / 820 IC Separation Center III 6.5 Warranty and Conformity ...

3 Operation 819 IC Detector / 820 IC Separation Center 62 Auto Step * fill, inject, off Display of current auto step status. Entry field Set a

3.2 820 IC Separation Center 819 IC Detector / 820 IC Separation Center 63Time program The Program tab is only available for a 820.0XX0 Separation

3 Operation 819 IC Detector / 820 IC Separation Center 64 List of program instructions The following program instructions can be added to the tim

3.2 820 IC Separation Center 819 IC Detector / 820 IC Separation Center 65<On> Only active if the thermostat is off. Switch the thermostat o

4 Notes - Maintenance - Faults 819 IC Detector / 820 IC Separation Center 66 4 Notes - Mainte-nance - Faults 4.1 Practical notes on ion chromato

4.1 Practical notes on ion chromatography 819 IC Detector / 820 IC Separation Center 67Storage Always store the separating columns closed when not

4 Notes - Maintenance - Faults 819 IC Detector / 820 IC Separation Center 68 valves, pressure rise and in extreme cases to scratched pistons. It

4.2 Maintenance and servicing 819 IC Detector / 820 IC Separation Center 69Eluent change When the eluent is changed, it must be ensured that no pre

4 Notes - Maintenance - Faults 819 IC Detector / 820 IC Separation Center 70 Maintenance by Metrohm service Maintenance of the 819 IC Detector an

4.2 Maintenance and servicing 819 IC Detector / 820 IC Separation Center 714.2.5 Changing separating columns Identical separation system If you w

Table of contents 819 IC Detector / 820 IC Separation Center IV List of figures Fig. 1: Block diagram of the ion chromatography systems ...

4 Notes - Maintenance - Faults 819 IC Detector / 820 IC Separation Center 72 5 Remove coupling • Remove 6.2744.040 Coupling 71 between column

4.2 Maintenance and servicing 819 IC Detector / 820 IC Separation Center 733 Connect suppressor to IC system • Reconnect suppressor to the IC s

4 Notes - Maintenance - Faults 819 IC Detector / 820 IC Separation Center 74 6 Clean connection piece • Clean the sealing surface of connectio

4.2 Maintenance and servicing 819 IC Detector / 820 IC Separation Center 754.2.8 Replacement of suppressor module The suppressor in the suppresso

4 Notes - Maintenance - Faults 819 IC Detector / 820 IC Separation Center 76 6 Insert connection piece • Insert connection piece 73 in suppr

4.3 Faults and malfunctions 819 IC Detector / 820 IC Separation Center 774.3 Faults and malfunctions 4.3.1 Malfunctions and their rectification If

4 Notes - Maintenance - Faults 819 IC Detector / 820 IC Separation Center 78 No feed of regen-eration or rinsing solution for sup-pressor • Con

5.1 RS 232 interface 819 IC Detector / 820 IC Separation Center 795 Interfaces 5.1 RS 232 interface The RS 232 interface 9 of the 819 IC Detector

5 Interfaces 819 IC Detector / 820 IC Separation Center 80 5.1.2 Pin assignment RS 232 C interface external Transmitted Data (TxD) If no data

5.2 Remote interfaces 819 IC Detector / 820 IC Separation Center 815.2 Remote interfaces The 819 IC Detector has the two remote interfaces 8 "

1.1 Instrument description 819 IC Detector / 820 IC Separation Center 1 1 Introduction 1.1 Instrument description 1.1.1 819 IC Detector The 819 IC

5 Interfaces 819 IC Detector / 820 IC Separation Center 82 819 IC Detector Pin Function Outputs 5 Ready L = ready (program inactive or not

5.2 Remote interfaces 819 IC Detector / 820 IC Separation Center 835.2.2 "IC Separation Center" interface The 820 IC Separation Center i

5 Interfaces 819 IC Detector / 820 IC Separation Center 84 819 IC Detector Pin Function Outputs 5 Valve A → "FILL" Valve A is swi

5.3 Analog output 819 IC Detector / 820 IC Separation Center 85 5.3 Analog output Analog output 5 "Output“ (0…1 V) of the 819 IC Detector (se

5 Interfaces 819 IC Detector / 820 IC Separation Center 86 5.5 Valve interfaces The two valve interfaces 26 and 31 can be used to connect the 820

6.1 Technical data 819 IC Detector / 820 IC Separation Center 876 Appendix 6.1 Technical data Provided that nothing to the contrary is mentioned

6 Appendix 819 IC Detector / 820 IC Separation Center 88 Conductivity detector Construction Thermostatted conductivity detector with 2 ring-shap

6.1 Technical data 819 IC Detector / 820 IC Separation Center 89Safety specifications Construction/testing According to EN/IEC 61010-1 / UL 3101-

6 Appendix 819 IC Detector / 820 IC Separation Center 90 Height 130 mm Depth 343 mm Weight 8.2 kg (with detector block, without accessories)

6.1 Technical data 819 IC Detector / 820 IC Separation Center 91 Immunity to interference Standards met: - EN/IEC 61326 - EN/IEC 61000-4-2 - EN/I