Metrohm 714 IC Metrodata Manuel d'utilisateur

METROHM Ltd. CH-9101 Herisau Switzerland Phone ++41 71 353 85 85 Fax ++41 71 353 89 01 8.714.8053Short Operating GuideIC Metrodata for Win95

2 Installation IC Metrodata for Win95 4 Connect IC system 1 1) Connect 6.2128.140 cable to socket 1 (channel 1) of the PC board. 2) Connect the

2.2 Software installation IC Metrodata for Win95 5 2.2 Software installation The installation program copies the files from the installation disk

2 Installation IC Metrodata for Win95 6 2.3 First program start Double-click the software icon to start the program. The program window with th

2.4 Security system IC Metrodata for Win95 7 2.4 Security system The «IC Metrodata for Win95» program has a security system based on the list of us

2 Installation IC Metrodata for Win95 8 2.5 Interface configuration Open the menu item Options / Interfaces for configuration of the inter-faces

3.1 General remarks IC Metrodata for Win95 9 3 Learning by doing 3.1 General remarks Main menu After starting the "IC Metrodata for Win95&q

3 Learning by doing IC Metrodata for Win95 10 3.2 Developing a new method This section describes the procedure how to develop a new, user-specif

3.2 Developing a new method IC Metrodata for Win95 11 • Set injection valve at 733 IC Separation Center to "FILL" (manually or by progra

3 Learning by doing IC Metrodata for Win95 12 Enter components for calibration • Click on or select Calibration / Components of the Method

3.2 Developing a new method IC Metrodata for Win95 13 Enter concentrations for calibration • When all components have been entered click the Conce

3 Learning by doing IC Metrodata for Win95 14 Start calibration • Click the Calibrate button. The Recalibration window appears. • Select the d

3.2 Developing a new method IC Metrodata for Win95 15 Set processing options • Click on or select Method setup of the Method menu. Select the

3 Learning by doing IC Metrodata for Win95 16 Report output to screen • Click on or select Make report of the Process menu. The Report Optio

3.2 Developing a new method IC Metrodata for Win95 17 A report can also be printed out without preceding screen output: • Click on or select

3 Learning by doing IC Metrodata for Win95 18 • Open the Peak Label tab. • Select the desired peak label. The Baseline Marker option for dis

3.2 Developing a new method IC Metrodata for Win95 19 Change report options • Click on or select Report options of the Method menu. • Under I

3 Learning by doing IC Metrodata for Win95 20 Close chromatogram window • Close the chromatogram window. A window appears with the mes-sage Chan

3.2 Developing a new method IC Metrodata for Win95 21 2nd numeral: Code for month (1…9 = Jan. … Sept., a…c = Oct. … Dec.) 3rd+ 4th numeral: Day

3 Learning by doing IC Metrodata for Win95 22 3.3 Use of existing methods This section describes the procedure how to record, integrate and cali

3.3 Use of existing methods IC Metrodata for Win95 23 Preparations • Insert separating column in IC system and condition it. • Prepare standards

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3 Learning by doing IC Metrodata for Win95 24 • Before starting the sample determination, you have to calibrate and perhaps modify the method. T

3.3 Use of existing methods IC Metrodata for Win95 25 • If required, enter the time delay as Delay before starting peak inte-gration at the first

3 Learning by doing IC Metrodata for Win95 26 • If the Peak column contains a 0 the peak must be manually allocated to a component. In this case

3.3 Use of existing methods IC Metrodata for Win95 27 • Select the Level and click on the OK button. • Click the OK button in the Concentrations

3 Learning by doing IC Metrodata for Win95 28 • Set the injection valve at the 733 IC Separation Center to "INJECT" (manually or by pr

3.4 Multipoint calibration IC Metrodata for Win95 29 3.4 Multipoint calibration This section describes the procedure how to perform a calibration w

3 Learning by doing IC Metrodata for Win95 30 Record third to xth standard chromatogram • Click on or select Passport of the Method menu. •

3.4 Multipoint calibration IC Metrodata for Win95 31 Enter concentrations for calibration • Select Open method of the File menu. • Select the pre

3 Learning by doing IC Metrodata for Win95 32 Start calibration • Click on or select Open of the File menu. • Select all previously record

3.4 Multipoint calibration IC Metrodata for Win95 33 • Because the second up to the xth standard have been recorded as samples (0) the levels bel

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3 Learning by doing IC Metrodata for Win95 34 Modify calibration • Select Open method of the File menu. • Select the method used for calibratio

3.4 Multipoint calibration IC Metrodata for Win95 35 Save method • Select Save method as of the File menu. The File Save As window appears. • Cli

3 Learning by doing IC Metrodata for Win95 36 3.5 Modify several chromatograms This section describes the procedure for reintegrating, recalcula

3.5 Modify several chromatograms IC Metrodata for Win95 37 • Select the desired method for recalculation of all chromatograms recorded with this

3 Learning by doing IC Metrodata for Win95 38 3.6 Use of sample tables This section describes how to construct sample data tables with the aid o

3.6 Use of sample tables IC Metrodata for Win95 39 • Overwrite the fields of the second line with the data for the second sample. • Repeat this p

3 Learning by doing IC Metrodata for Win95 40 Start reprocessing • For reprocessing of the recorded chromatograms proceed accord-ing to section

3.7 Export data IC Metrodata for Win95 41 3.7 Export data This section describes how to export data via clipboard or report out-put for further pro

3 Learning by doing IC Metrodata for Win95 42 Export via file report • Click on or select Open of the File menu. • Select the desired chrom

3.7 Export data IC Metrodata for Win95 43 • If required, change the other report options (see section 3.2). Switch on the Chromatogram Plot option

Table of contents IC Metrodata for Win95 I Table of contents 1 Introduction ... 1 1.1

3 Learning by doing IC Metrodata for Win95 44 • In the Chromatograms acquired by method window, select the de-sired method for export of all the

3.7 Export data IC Metrodata for Win95 45 • Enter the directory for storage of the exported files in the Directory field. • Enter the name of the

3 Learning by doing IC Metrodata for Win95 46 3.8 Method associated remote control This section describes the procedure how to associate a time

3.8 Method associated remote control IC Metrodata for Win95 47 • First click to 732 IC Detector[ COM# ] an then click the Setup button.

3 Learning by doing IC Metrodata for Win95 48 • Select the IC system type in the Initial tab. With Anion and Cation temperature coefficient and

3.8 Method associated remote control IC Metrodata for Win95 49 Example for remote instructions and time program In the Remote configuration tab, th

3 Learning by doing IC Metrodata for Win95 50 Start cycle program and data acquisition • Click on or select Restart method of the Acquire me

3.8 Method associated remote control IC Metrodata for Win95 51 Start inject programm and data acquisition • Select Equipment of the Method menu. •

3 Learning by doing IC Metrodata for Win95 52 togram. Therefore, program and parameters can be changed dur-ing a running method, but the changes

3.9 Manual remote control IC Metrodata for Win95 53 3.9 Manual remote control This section describes the procedure how to send parameters and time

IC Metrodata for Win95 II

3 Bedienungslehrgang IC Metrodata for Win95 54 • Change the parameters for 732 IC Detector, 733 IC Separation Center and 709 IC Pump on the righ

3.9 Manual remote control IC Metrodata for Win95 55 Write, send and activate a program • Select Equipment setup of the Options menu. • In the Con

3 Bedienungslehrgang IC Metrodata for Win95 56 • Select Equipment setup of the Options menu. • In the Configured equipment control drivers wind

4.1 Software license IC Metrodata for Win95 57 4 Appendix 4.1 Software license The «IC Metrodata for Win95» program is installed as a full program

4 Appendix IC Metrodata for Win95 58

4.4 Index IC Metrodata for Win95 59 4.4 Index A Access levels...7 Analysis time ...

4 Appendix IC Metrodata for Win95 60 O On-Line display ...10,23,29,39,40 Open queue during data acquisition...39 Open recorde

1.1 General information IC Metrodata for Win95 1 1 Introduction 1.1 General information «IC Metrodata for Win95», the new evaluation tool consistin

2 Installation IC Metrodata for Win95 2 2 Installation Protection against static charges Electronic components are sensitive to static charging

2.1 Hardware installation IC Metrodata for Win95 3 Installation of 2nd PC Board (1.714.0310) 1) Switch off PC and disconnect power cable from powe