Metrohm 761 SD Compact IC Manuel d'utilisateur

761 SD Compact IC 8.761.1043Instructions for Use CH-9101 Herisau/Schweiz E-Mail [email protected] Internet www.metrohm.com

1 Introduction 761 SD Compact IC / Instructions for Use 8.761.1043 2 All components coming into contact with eluent and sample are metal-free. Re

6 Notes – Maintenance – Faults 761 SD Compact IC / Instructions for Use 8.761.1043 92 rinsed free of salt with methanol/water (1:4) to avoid cry

6.2 Maintenance and servicing 761 SD Compact IC / Instructions for Use 8.761.1043 931 Detach the pump head • Disconnect the "tubing con

6 Notes – Maintenance – Faults 761 SD Compact IC / Instructions for Use 8.761.1043 94 Figure 15: Components of the pump head Figure 16: Re

6.2 Maintenance and servicing 761 SD Compact IC / Instructions for Use 8.761.1043 95 24 Pump head 6.2824.100 68Screw for piston cartridge 72 69

6 Notes – Maintenance – Faults 761 SD Compact IC / Instructions for Use 8.761.1043 96 5 Clean/replace inlet valve 77 and outlet valve 78 • Cle

6.2 Maintenance and servicing 761 SD Compact IC / Instructions for Use 8.761.1043 97 Figure 17: Components of inlet valve 77 and outlet valve 7

6 Notes – Maintenance – Faults 761 SD Compact IC / Instructions for Use 8.761.1043 98 6.2.6 Regeneration of the suppressor module Regeneration o

6.2 Maintenance and servicing 761 SD Compact IC / Instructions for Use 8.761.1043 99Regeneration of the suppressor in the case of high counter-pr

6 Notes – Maintenance – Faults 761 SD Compact IC / Instructions for Use 8.761.1043 100 6.2.7 Cleaning the suppressor It may be necessary to clea

6.2 Maintenance and servicing 761 SD Compact IC / Instructions for Use 8.761.1043 1015 Insert the suppressor rotor • Insert the suppressor r

1.2 Parts and controls 761 SD Compact IC / Instructions for Use 8.761.1043 3 1.2 Parts and controls In this section you will find the numbers

6 Notes – Maintenance – Faults 761 SD Compact IC / Instructions for Use 8.761.1043 102 6.2.8 Replacing the suppressor The suppressor in the supp

6.2 Maintenance and servicing 761 SD Compact IC / Instructions for Use 8.761.1043 1037 Connect and condition the suppressor • Reconnect the

6 Notes – Maintenance – Faults 761 SD Compact IC / Instructions for Use 8.761.1043 104 6.3 Faults and malfunctions 6.3.1 Error messages If any ty

6.3 Faults and malfunctions 761 SD Compact IC / Instructions for Use 8.761.1043 105Malfunction Cause Rectification No feed of re-generation or

6 Notes – Maintenance – Faults 761 SD Compact IC / Instructions for Use 8.761.1043 106 6.4 Diagnostic tests / Validation / GLP The requirements

7.1 Technical data 761 SD Compact IC / Instructions for Use 8.761.1043 1077 Appendix 7.1 Technical data Unless otherwise specified, the publishe

7 Appendix 761 SD Compact IC / Instructions for Use 8.761.1043 108 Max. temperature deviation ± 2.5°C Heating time ≥ 30 min Temperature stabili

7.1 Technical data 761 SD Compact IC / Instructions for Use 8.761.1043 109Pump displacement volumes Main piston: 28.5 µL Priming piston: 14.25

7 Appendix 761 SD Compact IC / Instructions for Use 8.761.1043 110 Pin assignment 7.1.9 Remote interface Connector Dsub 25 pin (female) Circui

7.1 Technical data 761 SD Compact IC / Instructions for Use 8.761.1043 1117.1.11 Safety specifications Construction/testing According to IEC/EN

1 Introduction 761 SD Compact IC / Instructions for Use 8.761.1043 4 1.2.2 Rear view Figure 2: Rear panel 761 SD Compact IC 8Opening for outlet

7 Appendix 761 SD Compact IC / Instructions for Use 8.761.1043 112 7.2 Standard equipment Subject to changes ! All dimensions are given in mm.

7.2 Standard equipment 761 SD Compact IC / Instructions for Use 8.761.1043 113Quant. Order No. Description 2.761.0420 2.761.0520 2 2 6.1816

7 Appendix 761 SD Compact IC / Instructions for Use 8.761.1043 114 Quant. Order No. Description 2.761.0420 2.761.0520 1 1 6.2027.040 Column

7.2 Standard equipment 761 SD Compact IC / Instructions for Use 8.761.1043 115Quant. Order No. Description 2.761.0420 2.761.0520 2 2 6.2621

7 Appendix 761 SD Compact IC / Instructions for Use 8.761.1043 116 Quant. Order No. Description 2.761.0420 2.761.0520 5 6 6.2744.010 PEE

7.2 Standard equipment 761 SD Compact IC / Instructions for Use 8.761.1043 117Quant. Order No. Description 2.761.0420 2.761.0520 1 1 6.28

7 Appendix 761 SD Compact IC / Instructions for Use 8.761.1043 118 7.3 Optional accessories 7.3.1 6.5328.000 SD Spare Part Set A specially selec

7.3 Optional accessories 761 SD Compact IC / Instructions for Use 8.761.1043 1191 6.2744.040 PEEK coupling For the connection of 1⁄16"-Capil

7 Appendix 761 SD Compact IC / Instructions for Use 8.761.1043 120 7.3.2 Other optional accessories Order No. Description 6.2321.010 MCAL Ch

7.4 Warranty and conformity 761 SD Compact IC / Instructions for Use 8.761.1043 1217.4 Warranty and conformity 7.4.1 Warranty The warranty on ou

1.2 Parts and controls 761 SD Compact IC / Instructions for Use 8.761.1043 5 1.2.3 Connection schematic Figure 3: Connection schematic for 761 S

7 Anhang 761 SD Compact IC / Gebrauchsanweisung 8.761.1043 122 7.4.2 Declaration of Conformity This is to certify the conformity to the standa

7.4 Warranty and conformity 761 SD Compact IC / Instructions for Use 8.761.1043 123 7.4.3 Quality Management Principles Metrohm Ltd., CH-9101 H

7 Appendix 761 SD Compact IC / Instructions for Use 8.761.1043 124 7.5 Index <Inject> ...45, 46 «IC Cap» ...

7.5 Index 761 SD Compact IC/ Instructions for Use 8.761.1043 125Detector block Connection ... 15 Detector block 40

7 Appendix 761 SD Compact IC / Instructions for Use 8.761.1043 126 for column holder Figure...41 Mounting rail 67

7.5 Index 761 SD Compact IC/ Instructions for Use 8.761.1043 127Reserve range ... 107 RESET...

1 Introduction 761 SD Compact IC / Instructions for Use 8.761.1043 6 32 Sample loop 1.5 µL (6.1825.240) PEEK sample loop 33 Column connection cap

1.3 Information on the Instructions for Use 761 SD Compact IC / Instructions for Use 8.761.1043 7 1.3 Information on the Instructions for Use P

1 Introduction 761 SD Compact IC / Instructions for Use 8.761.1043 8 1.3.2 Notation and pictograms The following notations and pictograms (symbol

1.4 Safety notes 761 SD Compact IC / Instructions for Use 8.761.1043 9 1.4 Safety notes 1.4.1 Electrical safety While electrical safety in the ha

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 10 2 Installation 2.1 Flow chart The following flow chart provides an overvie

2.2 Setting up the instrument 761 SD Compact IC / Instructions for Use 8.761.1043 112.2 Setting up the instrument 2.2.1 Packaging The 761 SD Com

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 12 2.3 Description of the connections 2.3.1 Connection of capillaries/tubing

2.3 Description of the connections 761 SD Compact IC / Instructions for Use 8.761.1043 13Figure 4: Connectors for ca-pillaries 2.3.2 Connection

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 14 Capillaries may also be connected together via PEEK inline filters, see Sec

2.4 Connection of the detector block 761 SD Compact IC / Instructions for Use 8.761.1043 152.4 Connection of the detector block The metal-free d

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 16 The inlet and outlet capillaries (39 and 41) to and from the detector bloc

2.6 Installing the eluent path 761 SD Compact IC / Instructions for Use 8.761.1043 172.6 Installing the eluent path 2.6.1 High-pressure pump –

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 18 2.6.3 Connection high-pressure pump → injection valve In order to protect

2.6 Installing the eluent path 761 SD Compact IC / Instructions for Use 8.761.1043 192.6.4 Connection injection valve → suppressor The precolumn

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 20 2.6.7 Connection suppressor → waste Route the "suppressor outlet capil

2.7 Installing the regenerant path 761 SD Compact IC / Instructions for Use 8.761.1043 21Figure 8: Pump tubing for regenerant path 57Tubing cart

CH-9101 Herisau/Schweiz E-Mail [email protected] Internet www.metrohm.com 761 SD Compact IC 8.761.1043 Instructions for Use 8.761.1043

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 22 3 Connection MPak pump tubing The regenerant MPak and pump tubing are co

2.8 Installing the sample path 761 SD Compact IC / Instructions for Use 8.761.1043 232.8 Installing the sample path The sample is aspirated with

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 24 Figure 10: Pump tubing for sample path 57 Tubing cartridge 58 Pressure l

2.8 Installing the sample path 761 SD Compact IC / Instructions for Use 8.761.1043 252 Connection pump tubing - injection valve • The sample

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 26 2.9 Connecting the 766 IC Sample Processor On instrument version 2.761.052

2.10 Fitting the rear panel 761 SD Compact IC / Instructions for Use 8.761.1043 272.10 Fitting the rear panel Now refit the rear panel which was

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 28 2.11 Mains connections Next connect the 761 SD Compact IC to the electrical

2.11 Mains connections 761 SD Compact IC / Instructions for Use 8.761.1043 29 Figure 13: Setting the mains voltage 2.11.2 Fuses One of the two f

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 30 2.12 Connection to the PC The next step is to connect the 761 SD Compact I

2.12 Connection to the PC 761 SD Compact IC / Instructions for Use 8.761.1043 313 Files The installation program copies the files from the inst

Teachware Metrohm AG Oberdorfstrasse 68 CH-9101 Herisau [email protected] 1. Edition 2004 These instructions are protected by copyright. All r

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 32 Enter cell constant Now enter the cell constant (see Section 2.4) printed

2.12 Connection to the PC 761 SD Compact IC / Instructions for Use 8.761.1043 332.12.4 Basic settings «IC Cap» Logging in The first time you sta

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 34 2.13 Deaerating the pump and rinsing the pulsa-tion dampener The high-pre

2.13 Deaerating the pump and rinsing the pulsation dampener 761 SD Compact IC / Instructions for Use 8.761.1043 353 Open the control window •

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 36 1 Detach the column connection capillary 33 from the PEEK coupling • U

2.14 Rinsing before fitting the column 761 SD Compact IC / Instructions for Use 8.761.1043 372.14 Rinsing before fitting the column Before the c

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 38 6 Check for leaks • Check all capillaries and tubing and their connecti

2.15 Precolumn and separating column 761 SD Compact IC / Instructions for Use 8.761.1043 392.15 Precolumn and separating column 2.15.1 Metrosep

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 40 2.15.2 Metrosep A Supp 1 HS separating column Now fit the supplied Metrose

2.15 Precolumn and separating column 761 SD Compact IC / Instructions for Use 8.761.1043 41 Figure 14: Connection of precolumn and separating c

Table of contents 761 SD Compact IC / Instructions for Use 8.761.1043 I Table of contents 1 Introduction ...

2 Installation 761 SD Compact IC / Instructions for Use 8.761.1043 42 2.16 Attaching tubing to side panels If required, the two "tubing con

3.1 «IC Net» – User interface for the 761 SD Compact IC 761 SD Compact IC / Instructions for Use 8.761.1043 433 «IC Net» The 761 SD Compact IC ca

3 «IC Net» 761 SD Compact IC / Instructions for Use 8.761.1043 44 3.1.3 Opening a method The method linked to the system can be opened by doub

3.1 «IC Net» – User interface for the 761 SD Compact IC 761 SD Compact IC / Instructions for Use 8.761.1043 453.1.5 Instrument icon System d

3 «IC Net» 761 SD Compact IC / Instructions for Use 8.761.1043 46 Conductivity, µS/cm Display of the currently measured conductivity. Pressure,

3.1 «IC Net» – User interface for the 761 SD Compact IC 761 SD Compact IC / Instructions for Use 8.761.1043 47Peristaltic pump Peristaltic pump &

3 «IC Net» 761 SD Compact IC / Instructions for Use 8.761.1043 48 The Program page contains the following two subpages: Program Main program wit

3.1 «IC Net» – User interface for the 761 SD Compact IC 761 SD Compact IC / Instructions for Use 8.761.1043 49Remote 0, 1, *, p Set remote outpu

3 «IC Net» 761 SD Compact IC / Instructions for Use 8.761.1043 50 Polarity Selection of the polarity for the output signal: + Positive polarity

3.1 «IC Net» – User interface for the 761 SD Compact IC 761 SD Compact IC / Instructions for Use 8.761.1043 51 Remote lines after power on The ou

Table of contents 761 SD Compact IC / Instructions for Use 8.761.1043 II 2.12 Connection to the PC ...

3 «IC Net» 761 SD Compact IC / Instructions for Use 8.761.1043 52 lution with a known conductivity through the IC system. Observe the displayed c

3.1 «IC Net» – User interface for the 761 SD Compact IC 761 SD Compact IC / Instructions for Use 8.761.1043 53PowerOn values Display of the valu

3 «IC Net» 761 SD Compact IC / Instructions for Use 8.761.1043 54 3.2 Systems supplied 3.2.1 System "startup.smt" System startup.smt i

3.2 Systems supplied 761 SD Compact IC / Instructions for Use 8.761.1043 55Configuration tab Same settings as in the example with system manual.s

3 «IC Net» 761 SD Compact IC / Instructions for Use 8.761.1043 56 3.2.3 System "auto.smt" System auto.smt is used for automatic measur

3.2 Systems supplied 761 SD Compact IC / Instructions for Use 8.761.1043 57Manual tab - Manual subwindow For manual control of the 766 IC Sample

3 «IC Net» 761 SD Compact IC / Instructions for Use 8.761.1043 58 Program tab Time program of the 766 IC Sample Processor. Configuration tab – R

3.2 Systems supplied 761 SD Compact IC / Instructions for Use 8.761.1043 59Configuration tab - Vial positions subwindow Configuration tab - Need

3 «IC Net» 761 SD Compact IC / Instructions for Use 8.761.1043 60 Configuration tab - Control subwindow Configuration tab - Scan subwindow

3.2 Systems supplied 761 SD Compact IC / Instructions for Use 8.761.1043 61Links tab Always connect the 766 IC Sample Processor to COM2. Linked

Table of contents 761 SD Compact IC / Instructions for Use 8.761.1043 III 6.2 Maintenance and servicing ...

3 «IC Net» 761 SD Compact IC / Instructions for Use 8.761.1043 62 System window System parameters Control tab Same settings as in the example wi

3.2 Systems supplied 761 SD Compact IC / Instructions for Use 8.761.1043 63Linked method Method SD_shutdown.mtw is linked to system shutdown.smt.

4 «IC Cap» 761 SD Compact IC / Instructions for Use 8.761.1043 64 4 «IC Cap» The 761 SD Compact IC can be operated via «IC Net» (see Section 3) o

4.1 «IC Cap» introduction 761 SD Compact IC / Instructions for Use 8.761.1043 65Frame: A sample parameter window, a chromatogram window or a re-s

4 «IC Cap» 761 SD Compact IC / Instructions for Use 8.761.1043 66 4.2 «IC Cap» - Configuration Clicking with the right mouse button (anywhere on

4.2 «IC Cap» - Configuration 761 SD Compact IC / Instructions for Use 8.761.1043 67Settings of configuration "manual.cfg" General tab

4 «IC Cap» 761 SD Compact IC / Instructions for Use 8.761.1043 68 On the Items tab, you can select which sample parameters are to be displayed in

4.2 «IC Cap» - Configuration 761 SD Compact IC / Instructions for Use 8.761.1043 69Limits tab With None as Action, there is only a warning enter

4 «IC Cap» 761 SD Compact IC / Instructions for Use 8.761.1043 70 In the case of two systems a prompt is displayed each time before starting the

4.2 «IC Cap» - Configuration 761 SD Compact IC / Instructions for Use 8.761.1043 71Main page with configuration "manual.cfg"

Table of contents 761 SD Compact IC / Instructions for Use 8.761.1043 IV List of figures Figure 1: Front of the 761 SD Compact IC ...

4 «IC Cap» 761 SD Compact IC / Instructions for Use 8.761.1043 72 4.2.3 Configuration "auto.cfg" Configuration auto.cfg should be loade

4.2 «IC Cap» - Configuration 761 SD Compact IC / Instructions for Use 8.761.1043 73Items tab On the Items tab, you can select which sample param

4 «IC Cap» 761 SD Compact IC / Instructions for Use 8.761.1043 74 Queue tab If Shut down system at the end is activated, no additional step is r

4.2 «IC Cap» - Configuration 761 SD Compact IC / Instructions for Use 8.761.1043 75Limits tab With None as Action, there is only a warning enter

4 «IC Cap» 761 SD Compact IC / Instructions for Use 8.761.1043 76 Miscellaneous tab The Report Timeout must be longer than 30 minutes. Otherwise

5.1 Operation with manual sample change 761 SD Compact IC / Instructions for Use 8.761.1043 775 Operation This section describes day-to-day oper

5 Operation 761 SD Compact IC / Instructions for Use 8.761.1043 78 2 Condition the instrument for 30 minutes ⇒ Insert the free end of the sam

5.1 Operation with manual sample change 761 SD Compact IC / Instructions for Use 8.761.1043 792 Calibration ⇒ Dry off the free end of the sam

5 Operation 761 SD Compact IC / Instructions for Use 8.761.1043 80 3 Sample determination ⇒ System manual.smt (see Section 3.2.2) should stil

5.1 Operation with manual sample change 761 SD Compact IC / Instructions for Use 8.761.1043 812 Allow shutdown.smt to run ⇒ Insert the free e

1.1 Instrument description 761 SD Compact IC / Instructions for Use 8.761.1043 1 1 Introduction 1.1 Instrument description The 761 SD Compact

5 Operation 761 SD Compact IC / Instructions for Use 8.761.1043 82 5.1.2.2 Calibration and sample determination (manual operation / «IC Cap») T

5.1 Operation with manual sample change 761 SD Compact IC / Instructions for Use 8.761.1043 833 Sample determination ⇒ Click on the yellow <

5 Operation 761 SD Compact IC / Instructions for Use 8.761.1043 84 5.2 Operation with automated sample change The instrument must have been con

5.2 Operation with automated sample change 761 SD Compact IC / Instructions for Use 8.761.1043 855.2.1.2 Creating the sample table (automated op

5 Operation 761 SD Compact IC / Instructions for Use 8.761.1043 86 5.2.2 Control with «IC Cap» (automated operation) Start the «IC Cap» software

5.2 Operation with automated sample change 761 SD Compact IC / Instructions for Use 8.761.1043 87Example of a sample table: ⇒ If Shut down syste

6 Notes – Maintenance – Faults 761 SD Compact IC / Instructions for Use 8.761.1043 88 6 Notes – Maintenance – Faults 6.1 Practical notes on ion

6.1 Practical notes on ion chromatography 761 SD Compact IC / Instructions for Use 8.761.1043 89Maintenance An unstable baseline (pulsation and f

6 Notes – Maintenance – Faults 761 SD Compact IC / Instructions for Use 8.761.1043 90 The suppressor module must never be switched in dry state

6.2 Maintenance and servicing 761 SD Compact IC / Instructions for Use 8.761.1043 916.2 Maintenance and servicing 6.2.1 General information Care