Metrohm 902 Titrando Manuel d'utilisateur

902 TitrandoManual8.902.8003EN / 2014-08-19

1.2 Instrument description￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭902 TitrandoUp to three control instruments (Titrando, Dosing Interface, USB SampleProcessor,

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction902 Titrando￭￭￭￭￭￭￭￭31.3 Titration modes – Measuring modes – Dosing com-mandsThe 902 Titrando supports the follow

1.4 About the documentation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭902 Titrando1.4 About the documentationCAUTIONPlease read through this documentation carefu

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction902 Titrando￭￭￭￭￭￭￭￭5NOTEThis symbol highlights additional information andtips.1.5 Safety instructions1.5.1 Gene

1.5 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭902 TitrandoProtection against electrostatic chargesWARNINGElectronic components are sensitive t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument902 Titrando￭￭￭￭￭￭￭￭72 Overview of the instrument902 TitrandoiTrode readyOn21MetrohmFigure 2 Front

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭902 Titrando12345678910Figure 3 Rear 902 Titrando1Type plateContains specifications concerning supplyvoltage, instrumen

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation902 Titrando￭￭￭￭￭￭￭￭93 Installation3.1 Setting up the instrument3.1.1 PackagingThe instrument is supplied in hi

3.2 Connecting a controller￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭902 Titrando3.2.1.1 Connecting a Touch ControlNOTEThe plug is protected against accidental

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation902 Titrando￭￭￭￭￭￭￭￭11CAUTIONThe Touch Control must be shut down properly by deactivation withthe power switch on

3.2 Connecting a controller￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭902 Titrando6.2151.000Figure 5 Connecting the computerThe instrument is recognized. Dependi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation902 Titrando￭￭￭￭￭￭￭￭131Setting up the instrument￭ Start the PC software.The instrument is automatically recognized

3.3 Connecting MSB devices￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭902 TitrandoNOTEWhen connecting MSB devices together, the following must beobserved:￭ Only o

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation902 Titrando￭￭￭￭￭￭￭￭15Figure 7 Connecting a dosing device3.3.2 Connecting a stirrer or titration standYou can use

3.3 Connecting MSB devices￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭902 TitrandoFigure 8 Connecting an MSB stirrerFigure 9 Connecting the propeller stirrer to t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation902 Titrando￭￭￭￭￭￭￭￭17￭ Connect the Remote Box connection cable to one of the socketsmarked with MSB on the rear o

3.4 Connecting USB devices￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭902 Titrando3.4.2 Connecting a USB hubIf you wish to connect more than two devices to the U

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation902 Titrando￭￭￭￭￭￭￭￭19Figure 11 Connecting a printer3.4.4 Connecting a balance￭ Operation with a PC software:– Co

3.4 Connecting USB devices￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭902 TitrandoBalance CableMettler AE with interface option011 or 0126.2125.020 + 6.2125.010Al

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation902 Titrando￭￭￭￭￭￭￭￭21 2Switch on the Touch Control.The keyboard is recognized automatically and entered in the de

Metrohm AGCH-9100 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] TitrandoManual8.902.8003EN / 2014-08-

3.5 Connecting sensors￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭902 Titrando 4Program the barcode reader in such a way that the ASCII character02 (STX or Ctrl B

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation902 Titrando￭￭￭￭￭￭￭￭23NOTEThe electrode cable is protected against accidental disconnectionof the cable by means o

3.5 Connecting sensors￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭902 TitrandoNOTEAlways insert the red plug into the red socket. This is the only waythat shieldi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation902 Titrando￭￭￭￭￭￭￭￭25 2Plug in the electrode on the iConnect as illustrated below.Figure 16 Connecting an electro

4.1 General￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭902 Titrando4 Setting up the titration vessel4.1 GeneralDuring the titration, it is important that the so

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance902 Titrando￭￭￭￭￭￭￭￭275 Operation and maintenance5.1 General notes5.1.1 CareThe 902 Titrando requi

5.2 Quality management and qualification with Metrohm￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭902 Titrando5.2 Quality management and qualification withMetrohm

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting902 Titrando￭￭￭￭￭￭￭￭296 Troubleshooting6.1 GeneralProblem Cause RemedyThe "On" LED is notilluminate

6.2 SET titration￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭902 TitrandoProblem Cause Remedy￭ Select the user-defined titration rate anddecrease the control rang

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Appendix902 Titrando￭￭￭￭￭￭￭￭317 Appendix7.1 Remote interfaceThe 6.2148.010 Remote Box allows devices to be controlled which

TeachwareMetrohm AGCH-9100 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

7.1 Remote interface￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭902 TitrandoInputs+5 Vapprox. 50 kΩ Pull-uptp tp > 20 msactive = low, inactive = highOutputsOpe

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Appendix902 Titrando￭￭￭￭￭￭￭￭33Assignment Pin No. Function*Output 8 6 Output 9 7 Output 10 8 Output 11 13 Output 12 19 Out

7.1 Remote interface￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭902 TitrandoFunction ExplanationWarning The line is set for warning message display.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Technical specifications902 Titrando￭￭￭￭￭￭￭￭358 Technical specifications8.1 Measuring interfaceThe 902 Titrando has one galv

8.2 Power connection￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭902 TitrandoNTC 0.1 °CMeasuring accu-racyPt1000 ±0.2 °C(Applies for measuring range –20 - +150 °C;

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Technical specifications902 Titrando￭￭￭￭￭￭￭￭37￭ EN/IEC 61000-4-11￭ EN/IEC 61000-4-14￭ NAMUR8.5 Ambient temperatureNominal fun

8.8 Interfaces￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭902 TitrandoMSB connectors (Metrohm Serial Bus)Dosing device Connector for a maximum of four external do

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Warranty (guarantee)902 Titrando￭￭￭￭￭￭￭￭399 Warranty (guarantee)Metrohm guarantees that the deliveries and services it provid

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭902 TitrandoThe same warranty periods that are specified for a corresponding newpart apply to parts that are replaced

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10 Accessories902 Titrando￭￭￭￭￭￭￭￭4110 AccessoriesUp-to-date information on the scope of delivery and optional accessoriesfor yo

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents902 Titrando￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 The Titrando system ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭902 TitrandoThe Partslists webpage will be displayed. 7Select the desired output language. 8With the article number en

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Index902 Titrando￭￭￭￭￭￭￭￭43IndexNumbers/Symbols6.2151.000 controller cable ... 11685 Dosimat ... 1470

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭902 TitrandoUUpdateDevice software ... 2USBConnector ... 8USB connector

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭902 Titrando3.5.5 Differential potentiometry ... 2

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of figures902 Titrando￭￭￭￭￭￭￭￭VTable of figuresFigure 1 The Titrando system ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction902 Titrando￭￭￭￭￭￭￭￭11 Introduction1.1 The Titrando systemThe Titrando is the heart of the modular Titrando syst