Metrohm 797 VA Computrace Manuel d'utilisateur Page 257
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Noté. / 5. Basé sur avis des utilisateurs
8.7 Standard addition technique
797 VA Computrace – Software
245
Start determination.
8.7 Standard addition technique
Use manual standard addition without solution exchange
In the manual standard addition without solution exchange, a
known amount of the analyte is added once or several times to the
sample using a pipette. Proceed as follows:
1. Click on or MAIN WINDOW / Mode / Determination.
2. Click on or MAIN WINDOW / Window / Working method
specification
to open the WORKING METHOD SPECIFICATIONS
window.
3. Load the desired method into the WORKING METHOD SPECIFI-
CATIONS
window (see How to Load a method, section 8.4).
4. Select Standard addition in the Calibration field of the WORK-
ING METHOD SPECIFICATIONS
window.
5. Select
Manual in the Addition field of the WORKING METHOD
SPECIFICATIONS
window.
6. Select Batch in the Technique field of the WORKING METHOD
SPECIFICATIONS
window.
7. Click to open the EDIT WORKING METHOD PA-
RAMETERS
window.
8. Select the Determination tab (see section 5.2) and enter Sample
identifier
, Sample amount (not with the modes CVS and CPVS),
Cell volume, and the number of standard additions in the No. of
additions
field. (If you work with the CVS or CPVS mode, see
section 6.2
Calibration techniques with CVS and CPVS for a de-
scription of the parameters on the Determination tab).
9. Select the Substances tab (see section 5.2) and make sure that
for each substance entered in the table the number of the sin-
- 797 VA Computrace 1
- Table of contents 10
- Table of contents 11
- 1 Introduction 13
- 1.2 General information 14
- 1.3 Installation 14
- 1.3 Installation 15
- 1 Introduction 16
- 1.5 Overview of file types 19
- 1.6 Context sensitive menus 20
- 2 Main window 21
- 2 Main window 22
- 2.3 File menu 24
- 2.3 File menu 25
- 2.4 Mode menu 27
- 2.5 Utility menu 28
- 2.6 User menu 28
- 2.6 User menu 29
- 2.7 Settings menu 32
- 2.7 Settings menu 33
- 2.8 Window menu 46
- 2.8 Window menu 47
- 3.1 Electrodes 48
- 3.1 Electrodes 49
- Drop size [ 1...9 ; 4 ] 50
- 3.2 VA measurement modes 52
- 3.2 VA measurement modes 53
- METHOD SPECIFICATIONS 54
- KING METHOD SPECIFICATIONS 56
- Normal pulse 58
- 3.3 Potentiostat 71
- 3.5 Graphical settings 76
- 3.5 Graphical settings 77
- Color of the line 81
- 4 Exploratory mode 82
- 4 Exploratory mode 84
- 4.3 Exploratory curves 86
- 4.3 Exploratory curves 87
- PLORATORY CURVES 97
- EXPLORA 97
- TORY SPECIFICATION 97
- 5 Determination mode 98
- 5 Determination mode 100
- 797 VA Computrace – Software 101
- 5.3 Monitor 120
- 5.3 Monitor 121
- 5.4 Determination curves 130
- 5.4 Determination curves 131
- 5.5 Results 141
- 5.5 Results 143
- Electrode test 145
- 5.6 Sample table 146
- 5.6 Sample table 147
- Voltammogram 154
- Chronoamperogram 154
- Minimum 157
- Recommended 157
- 6 Electroplating Bath VA 162
- Calibra 205
- Calibration 205
- Calibration tech 207
- 7 Manual control 209
- 7 Manual control 210
- 7.2 Dosing Device control 211
- 7.3 Pump control 212
- 7.4 Film deposition 213
- 7.5 Cleaning procedure 215
- 8 How to ...? 217
- 8.2 User rights 218
- DOSINOS window: 239
- Suppressor standard 247
- Rinsing solution 247
- Response curve) 253
- 8.10 Diagnostic procedures 265
- 9 Troubleshooting 269
- 9.4 Dosing Device problems 270
- 9 Troubleshooting 272
- AC – Alternating 273
- FICATION 273
- METHOD PARAMETERS 273
- 9.6 Voltammetric problems 274
- 9.6 Voltammetric problems 275
- Software license 288
- Software license 289
- Index 291
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